LCMS:Epimedii Herba - Revision history

Editor: moved LCMS:Epimedii to LCMS:Epimedii Herba

2011-02-15T05:54:20Z

moved LCMS:Epimedii to LCMS:Epimedii Herba

Editor at 07:11, 14 February 2011

2011-02-14T07:11:52Z

Editor: moved Epimedii LC-MS to LCMS:Epimedii

2011-02-14T05:33:27Z

moved Epimedii LC-MS to LCMS:Epimedii

Editor at 07:49, 10 February 2011

2011-02-10T07:49:52Z

Toyama at 04:34, 4 February 2011

2011-02-04T04:34:14Z

Toyama at 02:30, 2 February 2011

2011-02-02T02:30:03Z

Toyama at 02:26, 2 February 2011

2011-02-02T02:26:48Z

Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ES...

2011-02-02T02:26:17Z

New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS ES...

New page

==TIC==
[[Image:Linderae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]

==Analytical conditions==
{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || 4.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

{| class="wikitable" style="width:80%"
|-
| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
|-
| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
|-
| Column Temperature|| 40℃
|-
| Solvent A || 5 mM Ammonium acetate solution
|-
| Solvent B || acetonitrile
|-
| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
|-
| Source voltage || – 3.5 kV
|-
| Capillary temperature || 200 °C
|-
| Nebulizer gas || 1.5 l/min
|}

==LC-MS raw data==

===Linderae Radix LC-MS===
{{JCampViewer|Linderae LC-MS.gz}}

← Older revision		Revision as of 07:11, 14 February 2011
Line 1:		Line 1:
		+	{{LCMS/Header}}
	{{CrudeDrug/TIC		{{CrudeDrug/TIC
	\|TICFile=Epimedii LC-MS		\|TICFile=Epimedii LC-MS

@@ Line 1: / Line 1: @@
-==TIC==
+{{CrudeDrug/TIC
-[[Image:Epimedii LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]
+|TICFile=Epimedii LC-MS
-==Analytical conditions==
+{{CrudeDrug/LCMS/Pos
-{| class="wikitable" style="width:80%"
+|PInstrument =Shimadzu LC-IT-TOF MS ESI
-|-
+|PColumn     =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
-| Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)
+|PTemperature=40
-|-
+|PSolventA   =5 mM Ammonium acetate solution
-| Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)
+|PSolventB   =acetonitrile
-|-
+|PGradient   =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-| Column Temperature|| 40℃
+|PVoltage    =4.5
-|-
+|PCapillary  =200
-| Solvent A || 5 mM Ammonium acetate solution
+|PGas        =1.5
-|-
+}}
-| Solvent B || acetonitrile
-|-
-| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-|-
-| Source voltage ||  4.5 kV
-|-
-| Capillary temperature || 200 °C
-|-
-| Nebulizer gas || 1.5 l/min
-|}
-{| class="wikitable" style="width:80%"
+{{CrudeDrug/LCMS/Neg
-|-
+|NInstrument =Shimadzu LC-IT-TOF MS ESI
-| Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)
+|NColumn     =Waters Atlantis T3 (2.1 mm x 150 mm)
-|-
+|NTemperature=40
-| Column || Waters Atlantis T3 (2.1 mm x 150 mm)
+|NSolventA   =5 mM Ammonium acetate solution
-|-
+|NSolventB   =acetonitrile
-| Column Temperature|| 40℃
+|NGradient   =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
-|-
+|NVoltage    =-3.5
-| Solvent A || 5 mM Ammonium acetate solution
+|NCapillary  =200
-|-
+|NGas        =1.5
-| Solvent B || acetonitrile
+}}
-|-
-| Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)
 |-
-| Source voltage || – 3.5 kV
-|-
-| Capillary temperature || 200 °C
-|-
-| Nebulizer gas || 1.5 l/min
-|}
-−
-−
-−
-−
-==LC-MS raw data==
-−
-===Epimedii LC-MS===
-{{JCampViewer|Epimedii LC-MS.gz}}

← Older revision		Revision as of 04:34, 4 February 2011
Line 51:		Line 51:

	===Epimedii LC-MS===		===Epimedii LC-MS===
−	{{JCampViewer\|~~Linderae~~ LC-MS.gz}}	+	{{JCampViewer\|Epimedii LC-MS.gz}}

@@ Line 50: / Line 50: @@
 ==LC-MS raw data==
-===Linderae Radix LC-MS===
+===Epimedii LC-MS===
 {{JCampViewer|Linderae LC-MS.gz}}